Building materials are required for a wide range of construction work including carpentry, roofing, structural reinforcement, insulation, and plumbing. The particle size and particle shape of the raw materials influence quality and performance of the end product, and therefore require quality control by particle characterization. Microtrac analyzers are successfully used to determine the size and shape of various building materials.
Building materials range from naturally occurring substances such as rock, clay, sand, and wood to synthetic polymers and multiple combinations of both (composites). Concrete or mortar are for example mixtures of cement and aggregates like sand or gravel.
CAMSIZER X2 to potężny, niezwykle wszechstronny analizator wielkości i kształtu cząstek o szerokim zakresie pomiarowym, który łączy najnowocześniejszą technologię kamer z elastycznymi opcjami dyspersji. Opierając się na zasadzie dynamicznej analizy obrazu (ISO 13322-2), CAMSIZER X2 dostarcza precyzyjnych informacji o rozmiarze i kształcie cząstek proszków, granulek i zawiesin w zakresie pomiarowym od 0,8 μm do 8 mm.
CAMSIZER X2 wymusza przepływ cząstek przed układem optycznym o wysokiej rozdzielczości. Bardzo jasne, stroboskopowe źródła światła LED i dwie kamery cyfrowe o wysokiej rozdzielczości osiągają częstotliwość odświeżania ponad 300 obrazów na sekundę. Mierzone cząstki są analizowane w czasie rzeczywistym przez wydajne oprogramowanie. W ten sposób CAMSIZER X2 rejestruje obrazy setek tysięcy do kilku milionów cząstek z najwyższą dokładnością w ciągu zaledwie 1 do 3 minut.
CAMSIZER X2 zapewnia szeroki wybór informacji o cząstkach, co pozwala na kompleksową i rzetelną charakterystykę materiału próbki. Nadaje się do użytku w badaniach i rozwoju, a także do rutynowych zadań związanych z kontrolą jakości.
In most cases the particle size distribution of sand used in building materials is analyzed by sieve analysis. Microtrac's CAMSIZER series can replace this time-consuming and error-prone technique with a quicker, more reliable method that provides a higher resolution of particle size results as well as additional particle shape information.
Two types of sand taken from different locations, measured with the CAMSIZER X2. This sand is used as a layer in glass-reinforced plastic pipes to increase the stiffness. The reported size parameter is xc min (=particle width). The red curve is slightly bimodal. Sand with a wide size distribution can be more closely packed in the core of the pipe which gives the finished product a higher stability.
One sand sample that was measured by sieving (black) and by the CAMSIZER X2 using two different dispersion modules: the X-Fall module (green) and the X-Jet module (red). The results compare extremely well, proving that CAMSIZER X2 can match existing sieve analysis results. Hence, product specifications based on sieve analysis can remain unchanged when transitioning to a CAMSIZER system.
Limestone (calcium carbonate) is a raw material used in many products.
The particle size distribution as measured with the CAMSIZER X2 for a range of limestone grades.
The particle shape distribution results for the same collection of limestone samples. The reported shape parameter is sphericity, defined as: sphericity = 4 p A/ P2 where "A = Area of the particle projection" and "P = Perimeter length of the particle projection". The least round sample is Nr 6 (red), while the most round sample is Nr 4 (light blue).
Typical result from a particle size analysis of a plaster sample. The size range is fairly wide, ranging from 2 microns to about 1 mm. The graph shows the result of the CAMSIZER X2 in X-Jet mode, measured with a dispersion pressure of 150 kPa (red curve).
The plaster particles are agglomerating and “sticky”, thus the results of a conventional sieve analysis shows much coarser data (black curve), especially for the fine particles. However, if the particles are dispersed properly with an air jet sieve (AS 200 jet, blue curve), the results agree perfectly with the CAMSIZER X2.
Save and reliable detection of oversized particles are among the most important objectives of particle size analyis. For this purpose, Dynamic Image Analysis with the CAMSIZER X2 is the most powerful technique with unmatched accuracy.
Figure 6 shows a silicate sample that was analyzed with the CAMSIZER X2 using the X-Fall module. First, the original sample was measured and the size distribution was found to range from 5 μm to 100 μm (red curve). Then, 0.1 % of oversized (> 100 μm) particles were added and the sample was analyzed again (green curve). Finally, the experiment was repeated with 1 % oversize added (blue curve).
This silicate is used as raw material for the coating of tiles and oversized particles will result in a rough and uneven surface of the finished tile. The CAMSIZER X2 reliably detects the correct amount of oversize. Note that below 100 μm, where all samples are identical, the reproducibility is excellent!